Synthesis of 5-propyl-2- (3, 5-difluorophenyl) Pyrimidine

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Synthesis of 5-propyl-2- (3, 5-difluorophenyl) Pyrimidine
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                        JIANG Zhongliang,ZONG Jie,WU Yao,Duan HuiJIANG Zhongliang,ZONG Jie,WU Yao,Duan Hui

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Key words:fluorin-containing phenyl pyrimidine derivative; liquid crystal; synthesis

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[1]JIANG Zhongliang,ZONG Jie,WU Yao,Duan Hui.Synthesis of 5-propyl-2- (3, 5-difluorophenyl) Pyrimidine[J].Journal of Tongji University(Natural Science),2008,36(1):132-134.

[2]DA Yu,xia,LI Zheng,YANG Jing,ya.Synthesis of 5-aryloxymethylene-2-(3-tolyloxyacetylamido)-1,3,4-thiadiazoles[J].Journal of Northwest Normal University Natural Science (Bimonthly),2001,37(3):44-47.

[3]ZHOU Li,WEI Qu-xian,ZHANG Yu-hua,YANG Xiong,YANG Song.Synthesis of 3-(5-(substitudelythio)-1,3,4-oxadiazol-2-yl)-2H-Chromen-2-ones[J].Journal of Southwest Guizhou Teachers College for Nationalities,2012(6).

[4]Li Yongde,Wang Qian,Shi Donghui,Fang Fang.Synthesis of 5-n-pentyl-2-(4'-cyanophenyl) pyrimidine[J].Journal of Tsinghua University(Science and Technology),1992(6).

[5]XIA Yue-tao,XIAO Xin-rong,WANG Ying,JIA Xiao-peng,CHEN Chuan.Synthesis of 3-methyl-5-phenyl-(2-difluorophenyl)-2morpholinol Hydrochloride[J].Journal of Nanhua University(Science and Technology),2011,25(4):102-104.

[6]JI Chang-you,ZHENG Chang-zheng,CHANG Xiu-li,KUANG Xin-mou.Synthesis of (5-bromo-2-hydroxyphenyl)-(phenyl) methanone and Crystal Structure[J].Journal of Xi an University of Engineering Science and Technology,2009,23(1).

[7]TAN Xiaohong,SONG Xinjian,WANG Yangang.Synthesis and biological activity of N-[5-(3-pyridyl)-1, 3,4-thiadiazol-2-y1]-N''-(substituted phenyl)ureas[J].Journal of Central China Normal University(Natural Sciences),2008,42(1).

[8]GAO Hong-feng,KANG Wan-li,XU Bin,WU Xiao-yan,WANG Yong-jian.Synthesis and crystal structure of 4-hydroxy-4-(2-(prop-2-ynyloxy)phenyl)butan-2-one[J].Journal of Northeast Normal University (Natural Science Edition),2010,42(3).

[9]LI Gui-ying,CHEN Ying-chun,ZHAO Shuang,MI Hao-yu,WANG En-si.Synthesis of 3-Methyl-1-(2-(1-piperidinyl)phenyl)butylamine[J].Journal of Jilin University: Sci Ed,2007,45(1):135-137.

[10]ZHANG Shi-ying,LIU Hong,WANG Jie.Synthesis of 4-[p- (methylsulfonyl) phenyl]-3-cycloxylfuran-2 (5H)-one[J].Journal of Shanghai Normal University(Natural Sciences),2004,33(2):70-72.

[11]TANG Qing-gang,JI Chun-xiang,ZHANG Dong-mei,YAN Yuan-hai,GUO Cheng.Synthesis and crystal structure of 4,4-(-2-fluorophenyl)-bis(3-methyl-1-phenyl-5-pyrazolyl) methane ethylate[J].Journal of Nanjing University of Technology,2006,28(6):86-90.

[12]BI Xiu-cheng,LI De-jiang,FU He-qing.Synthesis of 2-Aryl-3- N-Propanoyl-5- (4-Iodophenyl)- 1, 3, 4-Oxadiazolines[J].Journal of Jiangxi Normal University (Natural Sciences Edition),2007,31(1).

[13]谭小红,宋新建,汪焱钢.Synthesis and biological activity of N-[5-(3-pyridyl)-1, 3,4-thiadiazol-2-yl]-N''-(substituted phenyl)ureas[J].Journal of Central China Normal University(Natural Sciences),2008,42(1):62-64.

[14]LI Yun,HUANG Chang-jiang,GAO Hui,GAO Wei-na,LIU Deng-ke,XU Wei-ren,DU Qi-shi,WEI Dong-qing.Synthesis of (R)-N- [[3- [3-Fluoro- 4-morpholinyl ] phenyl ]- 2-oxo- 5-oxazolidinyl ]Methanol[J].Journal of Tianjin Normal University(Natural Science Edition),2005,25(4):13-15.

[15]ZHU Song-ling,LI Yan,WANG Zhong-wei.Synthesis, crystal structure and spectra characters of 2-(2,4-dichloro-5-floro-benzoly)-3-(4- chlorolphenyl)-4-(1,2,4-triazole-1-yl)-5-anilino-thiopene[J].Journal of Shandong University,2005,40(2):96-100.

[16]HUANG Qin,QIN Zhang-lan.Synthesis and fungicidal activity of 1-[5-(4-methoxy- phenyl)-1,3,4-oxadiazole-2-yl]-3-substituted benzoyl-thiourea[J].Journal of Central China Normal University(Natural Sciences),2005,39(1):64-66.

[17]DU Hong,guang,HAN Ke,fei,WANG Tao,LI Zheng,he,SHI Shu,jian,LIU Qun,ZHANG Shi,wei.Synthesis,characterization and crystal structure of 3-(2-ferrocenylethyl)-2-ferrocenoylfuran[J].Journal of Beijing University of Chemical Technology,2002,29(4):54-58.

[18]SHI Shao-min,LV Yin-hua,CHENG Yin-fang.Synthesis characterization and crystal structure of 2'-(2-picolinamido) phenyl benzoate[J].Journal of Hubei Normal University(Natural Science),2011,31(2).

[19]SHI Shao-min,LV Yin-hua,CHENG Yin-fang.Synthesis characterization and crystal structure of 2′-(2-picolinamido) phenyl benzoate[J].Journal of Hubei Normal University(Natural Science),2011(2):10-13.

[20]Lu Lu,Xu Suoping,Xu Guo,Yao Baiquan,Gu Xiaofang.Microwave solid phase synthesis and crystal structure of benzoic acid 3-hydroxy-4-(3-hydroxy-3-phenylacryloyl)phenyl benzoate-zinc(Ⅱ) complex[J].Journal of Xuzhou Normal University(Natural Science Edition),2012(1):57-60.

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JIANG Zhongliang, ZONG Jie, WU Yao, Duan Hui. Synthesis of 5-propyl-2- (3, 5-difluorophenyl) Pyrimidine[J].同济大学学报(自然科学版),2008,36(1):132~134

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Received:February 21,2006
Revised:February 21,2006
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