Analysis of Degradation Intermediates of Phenol with Potassium Ferrate by Gas Chromatography and Mass Spectrometry

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Analysis of Degradation Intermediates of Phenol with Potassium Ferrate by Gas Chromatography and Mass Spectrometry
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                        DENG ZifengDENG Zifeng
Department of Chemistry, Tongji University, Shanghai 200092, China
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YANG XiaoYANG Xiao
Department of Chemistry, Tongji University, Shanghai 200092, China
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XU WeiXU Wei
Department of Chemistry, Tongji University, Shanghai 200092, China
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Abstract:

The phenol was oxidized by potassium ferrate.The intermediates were extracted from the degraded mixtures with vaporization,derivation,and ionexchange methods and analyzed with gas chromatography and mass spectrometry(GCMS)techniques.Benzoquinone,hydroquinone,diaphenol,phenoxyl phenol,maleic acid,fumaric acid,and oxalic were determined.Based on the results，the degrading path of phenol was deduced.

Key words:potassium ferrate; gas chromatographymass spectrometry; phenol

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DENG Zifeng, YANG Xiao, XU Wei. Analysis of Degradation Intermediates of Phenol with Potassium Ferrate by Gas Chromatography and Mass Spectrometry[J].同济大学学报(自然科学版),2009,37(3):

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